320084 PR Drug Synthesis - Laboratory Course (2007W)
(5 courses)
Continuous assessment of course work
Labels
Beginn am 16.10.2007
Blocklehrveranstaltung 16.10.2007-29.11.2007
Blocklehrveranstaltung 16.10.2007-29.11.2007
Details
Language: German
Lecturers
- Helmut Spreitzer
- Barbara Datterl
- Christiane Egyed
- Miriam Emich
- Norbert Haider
- Wolfgang Holzer
- Sabine Leber
- Eva Schirmer
- Manochehr Shahabi Mohammad Shahi
- Karem Shanab
Classes
Currently no class schedule is known.
Information
Aims, contents and method of the course
Assessment and permitted materials
Minimum requirements and assessment criteria
The objective of the course is to teach the student in experimental techniques used in organic synthesis. This is illustrated by a number of important organic reactions. Practical training is given in this laboratory course.
Examination topics
Reading list
Association in the course directory
A202
Last modified: Fr 31.08.2018 08:57
Program: Separation of a mixture of two liquid compound by fractionated distillation under atmospheric pressure and diminished pressure; purification of a contaminated solid compound; isolation of an org. acid or base, respectively, by extraction.
Eight syntheses: Reactions of carboxylic derivatives (esterification, acetylation); reactions of carbonyl compounds (acetals-, imines-, enamines- und oximes); condensation and addition ractions and rearrangement reaction (Aldol-, Knoevenagel-, Mannich-, Perkin-, Diels-Alder-reactions, benzilic acid rearrangement reaction); reductions (komplex hydrides) and oxidation reactions; syntheses of heterocyclic and aromatic compounds; Grignard-reactions (use of septum and syringe; nitrogen atmosphere); preparation of drugs.