270108 VO Analytical Chemistry II (2010W)
Labels
Mo 10.00 - 11.00 Uhr c.t.(Prof.Dickert), Di, Do 11.00 - 12.00 Uhr c.t., HS II (Di: Prof.Lindner/Prof.Lämmerhofer, Do: Prof.Rizzi)
Beginn: 05.10.2010
Beginn: 05.10.2010
Details
Language: German
Examination dates
- Monday 17.01.2011
- Monday 24.01.2011
- Tuesday 01.02.2011
- Monday 07.02.2011
- Tuesday 15.02.2011
- Thursday 03.03.2011
- Thursday 03.03.2011
- Tuesday 12.04.2011
- Thursday 19.05.2011
- Thursday 19.05.2011
- Thursday 19.05.2011
- Thursday 30.06.2011
- Monday 04.07.2011
- Monday 11.07.2011
- Monday 29.08.2011
- Monday 05.09.2011
- Monday 05.09.2011
- Thursday 29.09.2011
- Friday 11.11.2011
- Friday 11.11.2011
- Monday 14.11.2011
- Monday 12.12.2011
- Monday 19.12.2011
- Monday 19.12.2011
- Thursday 12.01.2012
- Monday 23.01.2012
- Monday 06.02.2012
- Thursday 08.03.2012
- Thursday 26.04.2012
- Thursday 10.05.2012
- Thursday 31.05.2012
- Thursday 31.05.2012
- Thursday 31.05.2012
- Saturday 23.03.2013
Lecturers
Classes
Currently no class schedule is known.
Information
Aims, contents and method of the course
Assessment and permitted materials
Minimum requirements and assessment criteria
Theoretical fundamentals and applications of spectrometric methodsAims: Introduction into fundamentals of high performance separation methods, especially chromatography and electrophoresisAims: Discussion of fundamentals of mass spectrometry, comprising physical aspects of measurements (ionization, mass analysis) as well as chemical information in the spectra.
Examination topics
Beurteilung (LP): mündliche und schriftliche Prüfung
Reading list
M. Otto, "Analytische Chemie", VCH Weinheim; R. Kellner et al (eds.), "Analytical Chemistry", FECS Curriculum, Wiley - VCH
B. H. Budzikiewicz, "Massenspektrometrie, Eine Einführung", VCH Verlagsges.
F. Lottspeich: "Bioanalytik"
B. H. Budzikiewicz, "Massenspektrometrie, Eine Einführung", VCH Verlagsges.
F. Lottspeich: "Bioanalytik"
Association in the course directory
2LA-Ch 31
Last modified: We 19.08.2020 08:06
Atomic spectroscopy: AAS - graphite tube, flame, Zeeman effect, atomisation, modifiers - matrix effects; ICP-AES - properties of plasma, dynamic range, sample preparation; applications in environmental analysis, comparison with ICP-MS;
Fluorescence: sensitivity, two dimensional techniques, quenching mechanisms; detection of oxygen, polycyclic aromatic compounds, used oils;
Photoacoustics: basic principles, depth profiles, medical applications;
FT-IR: basic principles, NIR and MIR, coupling, gas phase detection and multireflection spectroscopy, adsorption phenomena and catalysis, NIR for refuse sorting, pattern recognition;
Interfacial spectroscopy: photoelectron spectroscopy, XPS-UPS, ESCA, Auger spectroscopy,
X-ray fluorescence analysis - multielement analysis, chemical effects, matrix effects, applications: steel production, authenticity of arts products.Contents: Fundamentals in chromatography and electrophoresis, theory and instrument setup of the most important separation methods: gas chromatography, liquid chromatography (including size exclusion, affinity and ion chromatography), capillary electrophoresis. Introduction into the theory of chromatography and electrophoresis: selectivity and efficiency. System setup of GC and LC: sample input, columns, detectors. Problem solving by GC, planar Chromatography and HPLC. Modern CE.Contents: Mass Spectrometry - an analytical tool; instrumentation (ionization, mass analyzers, detectors, vaccuum systems); data analysis; chemical structure information and fragmentation paths; typical applications: MS coupled with separation systems (GC-MS, HPLC-MS); MS in bioanalytics and proteomics research.