270108 VO Analytical Chemistry II (2011W)
Labels
Mo 10.00 - 11.00 Uhr c.t., Di, Do 11.00 - 12.00 Uhr c.t., Joseph Loschmidt Hörsaal.
Beginn: 06.10.2011
Beginn: 06.10.2011
Details
Language: German
Examination dates
Thursday
12.01.2012
Tuesday
28.02.2012
Thursday
08.03.2012
Tuesday
13.03.2012
Friday
30.03.2012
Thursday
19.04.2012
Thursday
19.04.2012
Thursday
26.04.2012
Thursday
26.04.2012
Thursday
26.04.2012
Thursday
26.04.2012
Thursday
26.04.2012
Thursday
10.05.2012
Friday
25.05.2012
Friday
25.05.2012
Thursday
31.05.2012
Thursday
31.05.2012
Thursday
31.05.2012
Thursday
31.05.2012
Thursday
21.06.2012
Wednesday
27.06.2012
Wednesday
27.06.2012
Wednesday
27.06.2012
Tuesday
17.07.2012
Tuesday
17.07.2012
Thursday
19.07.2012
Thursday
06.09.2012
Thursday
27.09.2012
Thursday
27.09.2012
Friday
28.09.2012
Thursday
25.10.2012
Thursday
25.10.2012
Thursday
08.11.2012
Thursday
29.11.2012
Thursday
31.01.2013
Lecturers
Classes
Currently no class schedule is known.
Information
Aims, contents and method of the course
Assessment and permitted materials
Minimum requirements and assessment criteria
Theoretical fundamentals and applications of spectrometric methodsAims: Introduction into fundamentals of high performance separation methods, especially chromatography and electrophoresisAims: Discussion of fundamentals of mass spectrometry, comprising physical aspects of measurements (ionization, mass analysis) as well as chemical information in the spectra.
Examination topics
Beurteilung (LP): mündliche und schriftliche Prüfung
Reading list
M. Otto, "Analytische Chemie", VCH Weinheim; R. Kellner et al (eds.), "Analytical Chemistry", FECS Curriculum, Wiley - VCH
B. H. Budzikiewicz, "Massenspektrometrie, Eine Einführung", VCH Verlagsges.
F. Lottspeich: "Bioanalytik"
B. H. Budzikiewicz, "Massenspektrometrie, Eine Einführung", VCH Verlagsges.
F. Lottspeich: "Bioanalytik"
Association in the course directory
2LA-Ch 31
Last modified: We 19.08.2020 08:06
Atomic spectroscopy: AAS - graphite tube, flame, Zeeman effect, atomisation, modifiers - matrix effects; ICP-AES - properties of plasma, dynamic range, sample preparation; applications in environmental analysis, comparison with ICP-MS;
Fluorescence: sensitivity, two dimensional techniques, quenching mechanisms; detection of oxygen, polycyclic aromatic compounds, used oils;
Photoacoustics: basic principles, depth profiles, medical applications;
FT-IR: basic principles, NIR and MIR, coupling, gas phase detection and multireflection spectroscopy, adsorption phenomena and catalysis, NIR for refuse sorting, pattern recognition;
Interfacial spectroscopy: photoelectron spectroscopy, XPS-UPS, ESCA, Auger spectroscopy,
X-ray fluorescence analysis - multielement analysis, chemical effects, matrix effects, applications: steel production, authenticity of arts products.Contents: Fundamentals in chromatography and electrophoresis, theory and instrument setup of the most important separation methods: gas chromatography, liquid chromatography (including size exclusion, affinity and ion chromatography), capillary electrophoresis. Introduction into the theory of chromatography and electrophoresis: selectivity and efficiency. System setup of GC and LC: sample input, columns, detectors. Problem solving by GC, planar Chromatography and HPLC. Modern CE.Contents: Mass Spectrometry - an analytical tool; instrumentation (ionization, mass analyzers, detectors, vaccuum systems); data analysis; chemical structure information and fragmentation paths; typical applications: MS coupled with separation systems (GC-MS, HPLC-MS); MS in bioanalytics and proteomics research.