270132 UE Advanced Laboratory Course in Organic Chemistry (2024W)
Continuous assessment of course work
Labels
Registration/Deregistration
Note: The time of your registration within the registration period has no effect on the allocation of places (no first come, first served).
- Registration is open from Su 01.09.2024 08:00 to Su 15.09.2024 23:59
- Registration is open from Fr 04.10.2024 17:00 to Fr 18.10.2024 23:59
- Deregistration possible until Fr 18.10.2024 23:59
Details
max. 48 participants
Language: German
Lecturers
- Katharina Pallitsch
- Sergio Armentia Matheu
- Christoph Bendl
- Sebastian Fritz
- El Czar Galleposo
- Konstantin Günther
- Angela Hofmeister
- Hanspeter Kählig
- Emanuel Thomas Mahambo
- Teodora Moiseanu
- Terézia Morávková
- Nils Pellinger
- Liubov Rubicheva
- Philipp Salomon
- Nikolas Skoulikas
- Roberto Tinelli
- Milos Vavrik
- Sabela Vega Ces
- Uroš Vezonik
- Alexander Irran (Student Tutor)
- Fanny Kormout (Student Tutor)
- Slavka Prodanova (Student Tutor)
- Annika Schindler (Student Tutor)
- Sebastian Wagner (Student Tutor)
Classes (iCal) - next class is marked with N
Dates
18.11. 2024, 9:00-10:45 h: Introductory discussion and intro literature search, both groups! (HS4)20.11.2024, 13:15-14:30 h: Intro TLCs as techniques (SR 3), both groups!21.11.2024, 9:00 h: Working place take over in the lab room 4 (working place number to be communicated after the introductory discussion!) December group only!21.11.2024, 13:30-16:30 h: Safety introduction and NMR (HS3), both groups!Practical work December group!25.11. - 11.12., 9:00-18:00h (1 h lunch break)12.12.2024, 9:00 h: Working places handed back, December group only! 07.01.2025, 9:00 h: Working place take over in the lab room 4 (working place number to be communicated after the introductory discussion!) January group only!Practical work January group!
07.01.-23.01., 9:00-18:00h (1 h lunch break)24.01.2025, 9:00 h: Working places handed back, January group only! 31.01.2025, 12:00 h: last possible date to hand in theoretical example, both groups!This practical course will take place from 9:00 am until 6:00 pm in the opcoming two semesters due to construction works in one of the typically used course rooms.Preferences for one of these two possible courses will be taken into account whenever possible (polls to be performed after the official registration phase is over). Preferences of students with other overlapping courses (written statement of course head needed!) and care responsibilities will be taken into account first.
- N Monday 18.11. 09:00 - 10:45 Hörsaal 4 Chemie HP Währinger Straße 42
Information
Aims, contents and method of the course
Assessment and permitted materials
Preparation and characterization of 10 synthetic products + creation of a synthetic working procedure on paper. For each practical synthetic example a short oral exam (6 P max), protocol+literature search (4 P max) and practical skills (8 P max) will be evaluated (maximum 18 P per example in total). Additionally, up to 12 points can be reached for the writing of the theoretical synthetic procedure, 3 points can be obtained by completing an evaluation form concerning the performed examples and 3 point by completing a short exam on TLCs.
Minimum requirements and assessment criteria
Mandatory criteria for acceptance to the course: Lectures “Organische Chemie I” and “Chemisches Grundpraktikum IIB” as well as parallel registration for the “Proseminar in Organic Chemistry” are mandatory.Recommened: Basic knowledge in spectroscopy,To pass the course it is necessary to obtain a minimum of 134 points (out of 198 in total). Grading key: 0-133 P = nicht genügend (5), 134-149 P = genügend (4), 150-167 = befriedigend (3), 168-184 = gut (2), 185-198 = sehr gut (1)
Examination topics
Students are asked about techniques, methods and theoretical backgrounds necessary to work on the relevant tasks before the practical work.
Reading list
Script and material on Moodle
Association in the course directory
BA CH 11b
Last modified: We 06.11.2024 12:46
The objective of the course is to improve the participants' knowledge of synthetic organic chemistry. A combination of 11 single- or two-steps experiments will be performed. These will elaborate on topics such as working with lithium bases, pure elements (sodium, bromine) and handling toxic substances. During the course of these experiments, technical skills such as working at low temperatures, under inert conditions and using syringes will be trained. The prepared samples will be purified by procedures like extraction, distillation, chromatography or crystallization and the final products characterised by classical physical and/or modern spectroscopic methods. For selected examples a literature search, including on-line information retrieval will be performed with the aim to evaluate, adapt, and apply known synthetic procedures.