321016 VO Instrumental Pharmaceutical Analytics - B9 (2017W)

4.00 ECTS (2.00 SWS), SPL 32 - Pharmazie

Vorlesungszeiten: Montag - Freitag 09:45-11:15 Uhr HS 6
02.10.2017 - 20.10.2017
Fragestunde: 31.10.2017 11.30 - 13.00 Uhr HS 6

Prüfungstermine:
07.11.2017 08.00 Uhr HS 7+8
12.12.2017 11.30 Uhr HS 7+8
24.01.2018 08.00 Uhr HS 7+8
20.02.2018 09.45 Uhr HS 7+8

Details

Language: German

Examination dates

Lecturers

Wolfgang Holzer

Classes (iCal) - next class is marked with N

    
    Monday
    02.10.
    09:45 - 11:15
    UZA2 Hörsaal 6 (Raum 2Z227) 2.OG
    
    Tuesday
    03.10.
    09:45 - 11:15
    UZA2 Hörsaal 6 (Raum 2Z227) 2.OG
    
    Wednesday
    04.10.
    09:45 - 11:15
    UZA2 Hörsaal 6 (Raum 2Z227) 2.OG
    
    Thursday
    05.10.
    09:45 - 11:15
    UZA2 Hörsaal 6 (Raum 2Z227) 2.OG
    
    Friday
    06.10.
    09:45 - 11:15
    UZA2 Hörsaal 6 (Raum 2Z227) 2.OG
    
    Monday
    09.10.
    09:45 - 11:15
    UZA2 Hörsaal 6 (Raum 2Z227) 2.OG
    
    Tuesday
    10.10.
    09:45 - 11:15
    UZA2 Hörsaal 6 (Raum 2Z227) 2.OG
    
    Wednesday
    11.10.
    09:45 - 11:15
    UZA2 Hörsaal 6 (Raum 2Z227) 2.OG
    
    Thursday
    12.10.
    09:45 - 11:15
    UZA2 Hörsaal 6 (Raum 2Z227) 2.OG
    
    Friday
    13.10.
    09:45 - 11:15
    UZA2 Hörsaal 6 (Raum 2Z227) 2.OG
    
    Monday
    16.10.
    09:45 - 11:15
    UZA2 Hörsaal 6 (Raum 2Z227) 2.OG
    
    Tuesday
    17.10.
    09:45 - 11:15
    UZA2 Hörsaal 6 (Raum 2Z227) 2.OG
    
    Wednesday
    18.10.
    09:45 - 11:15
    UZA2 Hörsaal 6 (Raum 2Z227) 2.OG
    
    Thursday
    19.10.
    09:45 - 11:15
    UZA2 Hörsaal 6 (Raum 2Z227) 2.OG
    
    Friday
    20.10.
    09:45 - 11:15
    UZA2 Hörsaal 6 (Raum 2Z227) 2.OG
    
    Tuesday
    31.10.
    11:30 - 13:00
    UZA2 Hörsaal 6 (Raum 2Z227) 2.OG

Information

Aims, contents and method of the course

Aims: acquisition of basic knowledge regarding spectroscopic methods; applications focusing on pharmaceutical analytics (proof of identity, proof of purity, quantitative determinations), synthesis and structural elucidation

Content: basic principles of spectroscopic methods, ultraviolet-visible spectroscopy, infrared-spectroscopy, atomic absorption spectroscopy, atomic emission spectroscopy, fluorescence spectroscopy, mass spectrometry, X-ray structure analysis, NMR spectroscopy (1H, 13C, 2D); for each method: theoretical background, instrumentation, applications, scope and limitations.
Basic principles of electrochemical methods, potentiometry und potentiometric titrations, voltammetry, polarography, amperometry, coulometry; for each method: instrumentation, applications, scope and limitations

Assessment and permitted materials

Written examination (60 minutes), 10 questions (for instance multiple choice, calculations, drawings, open questions, ....). To achieve one point a correct and complete answer to a question is required. Grading key: 10 P (1), 9 P (2), 8 P (3), 7 P (3), 6 P (4), 0-5 P (5).

Resources permitted: none

Minimum requirements and assessment criteria

minimum requirement: 60% (6 points of 10 possible)

Examination topics

topics of the lecture and applications

Reading list

M. Hesse, H. Meier, B. Zeeh; Spektroskopische Methoden in der organischen Chemie, Georg Thieme Verlag, Stuttgart, 9. Auflage, 2016
G. Rücker, M. Neugebauer, G. G. Willems; Instrumentelle pharmazeutische Analytik, Wissenschaftliche Verlagsgesellschaft mbH Stuttgart, 5. Auflage, 2013
A. Dominik, D. Steinhilber; Instrumentelle Analytik, Deutscher Apotheker Verlag, Stuttgart, 2002
J. B. Lambert, S. Gronert, H. F. Shurvell, D. A. Lightner; Spektroskopie - Strukturaufklärung in der organischen Chemie, Pearson, München, 2. Auflage, 2012

Association in the course directory

A206, BA16

Last modified: Sa 02.04.2022 00:27